14. Nickel Plating Troubleshooting Decision Tree

START: Nickel deposit is unacceptable
|
+-- Does the part pass a water-break test before activation?
|   |
|   +-- NO --> Re-clean. Do not adjust plating chemistry yet.
|   |
|   +-- YES
|
+-- Is adhesion poor or is the deposit peeling?
|   |
|   +-- YES --> Identify substrate
|              |
|              +-- Stainless/passive alloy --> Verify validated activation + nickel strike
|              +-- Steel/copper/brass --> Review oxide removal, transfer delay, cleaning
|
+-- Is the defect concentrated on edges/corners?
|   |
|   +-- YES --> Check calculated current density, anode distance,
|              agitation, temperature and pH for high-current burning
|
+-- Is the defect concentrated in recesses/low-current areas?
|   |
|   +-- YES --> Check contacts, anode coverage, shielding,
|              solution movement and contamination/Hull-cell behavior
|
+-- Is the surface rough or nodular?
|   |
|   +-- YES --> Inspect filtration, anode bags, tank/rack cleanliness,
|              airborne dirt and precipitated solids
|
+-- Is the surface pitted?
|   |
|   +-- YES --> Observe for gas bubbles; check cleaning, agitation,
|              filtration and supplier-approved wetting control
|
+-- Is the deposit hazy, dull or dark across most of the load?
|   |
|   +-- YES --> Verify temperature, pH, current density and rectifier output
|              |
|              +-- All correct --> Run Hull cell / contamination investigation
|
+-- Did the problem begin immediately after an addition or process change?
    |
    +-- YES --> Stop further additions. Review lot, identity, quantity,
               process log and cross-contamination risk.

Troubleshooting order

Use this order to avoid wasting chemistry:

  1. Confirm substrate and preparation.
  2. Confirm electrical contact.
  3. Recalculate surface area/current density.
  4. Verify temperature and pH.
  5. Inspect anode placement.
  6. Observe agitation and gas release.
  7. Inspect filtration and particles.
  8. Review recent additions/process changes.
  9. Run comparative test panels/Hull cell.
  10. Investigate contamination analytically if needed.

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