14. Nickel Plating Troubleshooting Decision Tree
START: Nickel deposit is unacceptable
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+-- Does the part pass a water-break test before activation?
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| +-- NO --> Re-clean. Do not adjust plating chemistry yet.
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| +-- YES
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+-- Is adhesion poor or is the deposit peeling?
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| +-- YES --> Identify substrate
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| +-- Stainless/passive alloy --> Verify validated activation + nickel strike
| +-- Steel/copper/brass --> Review oxide removal, transfer delay, cleaning
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+-- Is the defect concentrated on edges/corners?
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| +-- YES --> Check calculated current density, anode distance,
| agitation, temperature and pH for high-current burning
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+-- Is the defect concentrated in recesses/low-current areas?
| |
| +-- YES --> Check contacts, anode coverage, shielding,
| solution movement and contamination/Hull-cell behavior
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+-- Is the surface rough or nodular?
| |
| +-- YES --> Inspect filtration, anode bags, tank/rack cleanliness,
| airborne dirt and precipitated solids
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+-- Is the surface pitted?
| |
| +-- YES --> Observe for gas bubbles; check cleaning, agitation,
| filtration and supplier-approved wetting control
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+-- Is the deposit hazy, dull or dark across most of the load?
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| +-- YES --> Verify temperature, pH, current density and rectifier output
| |
| +-- All correct --> Run Hull cell / contamination investigation
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+-- Did the problem begin immediately after an addition or process change?
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+-- YES --> Stop further additions. Review lot, identity, quantity,
process log and cross-contamination risk.
Troubleshooting order
Use this order to avoid wasting chemistry:
- Confirm substrate and preparation.
- Confirm electrical contact.
- Recalculate surface area/current density.
- Verify temperature and pH.
- Inspect anode placement.
- Observe agitation and gas release.
- Inspect filtration and particles.
- Review recent additions/process changes.
- Run comparative test panels/Hull cell.
- Investigate contamination analytically if needed.
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